One-dimensional and Two-dimensional NMR Spectra

Part I One-dimensional FT-NMR

・ ¹H-NMR Spectra of alpha-Santonin and Acetoxypachydiol Dibenzoate
・ ¹H-NMR of Methyl 9,12-Octadecadienoate
・ Spin Decoupling Difference Spectrum of beta-Ionone, Cholic Acid and Mosesin-2
・ NOE Difference Spectrum of beta-Ionone,Crenulacetal A, 20-Hydroxy-ecdysone Striatene and Ailanthone　
・ Spectrum of Bassianolide――Saturation Transfer
・ SPT (Selective Population Transfer) of beta-Ionone and Aspartic Acid
・ Broadband Proton Decoupling Spectrum of beta-Ionone
・ Off-resonance Proton Decoupling Spectrum of beta-Ionone and Isobutylaldehyde
・ Gated Proton Irradiation Spectrum of beta-Ionone
・ Inverse Gated Proton Decoupling Spectrum of beta-Ionone (No NOE)
・ Selective Proton Decoupling Spectrum of beta-Ionone
・ LSPD Spectrum of beta-Ionone and Salvilenone
・ INEPT Spectrum of beta-Ionone
・ DEPT Spectrum of beta-Ionone and Compactin
・ INEPT and DEPT Without Decoupling of beta-Ionone
・ T1 (Longitudinal Relaxation/Spin-lattice Relaxation) of beta-Ionone and Cholesteryl Acetate
・ Removal of Huge Signals (WEFT and Presaturation Methods)
・ 1-3-3-1 and JR Spectrum of Sucrose

Part II Two-dimensional FT-NMR

・ J-Resolved Spectrum of alpha-Santonin, Mugineic Acid, Semburin and Trichilin-A
・ Heteronuclear J-Resolved Spectrum of beta-Ionone
・ COSY Spectrum of Ethyl Acetate, beta-Ionone,Compactin, Chromazonarol, Albocycline, Adenanthin and Aphanamol-I
・ DCOSY Spectrum Emphasizing Long-range Coupling (Aphanamol-I)
・ COSY-45 Spectrum
・ Phase-sensitive DQF-COSY Spectrum of L-Aspartic Acid and Chromazonarol
・ HOHAHA Spectrum of Gramicidin S and Brevetoxin A
・ NOESY Spectrum of beta-Ionone, Ailanthone, Aphanamol-I and Chromazonarol
・ Phase-sensitive NOESY Spectrum of Ailanthone,Gramicidin S, DNA 12-mer and Bassanolide
・ ROESY (CAMELSPIN) Spectrum of Gramicidin S
・ H,C-COSY Spectrum of beta-Ionone, L-Menthol,Compactin, Aphanamol-I, Metasequoic Acid A and Methyl 2,3,5-tri-omicron-acetyl-beta-D-fucofuranoside
・ H,P-COSY Spectrum of Lipid A
・ Phase-sensitive H,C-COSY Spectrum of Strychnine
・ HMQC Spectrum of Strychnine
・ Long-range H,C-COSY Spectrum of beta-Ionone and Compactin
・ COLOC Spectrum of Dictyotalide B
・ HMBC Spectrum of Strychnine and Cyanoviridin RR
・ Relayed H,C-COSY of alpha-Santonin
・ Relayed H,C-COSY/HOHAHA of alpha-Santonin
・ 2D-INADEQUATE Spectrum of L-Menthol,Cholesteryl Acetate, Rotenone, Compound X and Brevetoxin B

Part III Principles of FT-NMR

1 FT-NMR

1.1 1 Pulse Experiment
1.2 Spin Decoupling
1.3 Spin Decoupling Difference Spectrum (SDDS)
1.4 Long-range Selective Proton Decoupling (LSPD)
1.5 Gated Decoupling and Inverse Gated Decoupling
1.6 NOE Difference Spectrum (NOEDS), Selective Population Transfer (SPT), and Saturation Transfer
1.7 Inversion Recovery (T1 Measurement), PRFT,WEFT
1.8 Spin Echo (T2 Measurement)
1.9 INEPT
1.10 DEPT
1.11 Selective Excitation : DANTE, Redfield 214, Jump and Return (JR), 1-3-3-1
1.12 INADEQUATE

2 Two-dimensional FT-NMR

2.1 J-Resolved Spectroscopy (¹H)
2.2 Heteronuclear J-Resolved Spectroscopy
2.3 COSY, COSY-45, PCOSY, DCOSY
2.4 H,X-COSY
2.5 NOESY
2.6 Phase-Sensitive NOESY
2.7 ROESY (or CAMELSPIN) and HOHAHA
2.8 RELAY
2.9 HMQC and HMBC
2.10 2D-INADEQUATE
2.11 Multiple-quantum Filter